한국원자력안전기술원 / 이현우, 채정석*
Abstract
A simple spontaneous deposition kit for 210Po determination using alpha spectrometry was newly designed, and polonium deposition characteristics under various physicochemical conditions were evaluated using it. The high-purity silver disc (99.99%) showed high deposition efficiencies of over 85.1% in the HCl concentration range of 0.01-6 M. Optimal physicochemical factors were determined to be a temperature of 90 °C, deposition time of 90 min, and the use of ascorbic acid as a reducing agent in an amount similar to that of the interfering element (Fe).
Affiliations
Hyeon-Woo Lee 1, Jung-Seok Chae 2
1Korea Institute of Nuclear Safety, 62 Gwahak-ro, Yuseong-gu, Daejeon, 34142, South Korea.
2Korea Institute of Nuclear Safety, 62 Gwahak-ro, Yuseong-gu, Daejeon, 34142, South Korea. Electronic address: jschae@kins.re.kr.
편집위원
Po-210의 경우 방사화학적 분리도 어려울 뿐 아니라 자발흡착에 대한 문제도 있어 신규개발된 키트가 유용히 활용되면 향후 분석이 용이해질 것으로 사료됨
2023-09-06 14:30:51